3-Bromo-1,1,2,2-tetrafluoropropane → HCID 178447728, 화합물

HRID 612329

반응식

HRID 612329 반응식
Br[C:2]1[CH:7]=[CH:6][C:5]([C:8]2[CH:13]=[CH:12][C:11]([O:14][Si](C(C)(C)C)(C)C)=[CH:10][CH:9]=2)=[CH:4][CH:3]=1.C([Si:27]1([C:34]2[CH:39]=[CH:38][CH:37]=[CH:36]C=2)[CH2:32][CH2:31][C:30](=O)[CH2:29][CH2:28]1)CCCC.Br[CH2:41][C:42]([F:47])([F:46])[CH:43]([F:45])[F:44]>>[CH2:34]([Si@H:27]1[CH2:28][CH2:29][C@H:30]([C:2]2[CH:3]=[CH:4][C:5]([C:8]3[CH:9]=[CH:10][C:11]([O:14][CH2:41][C:42]([F:47])([F:46])[CH:43]([F:45])[F:44])=[CH:12][CH:13]=3)=[CH:6][CH:7]=2)[CH2:31][CH2:32]1)[CH2:39][CH2:38][CH2:37][CH3:36]

참가 물질

4

반응물 3

HCID 696233-Bromo-1,1,2,2-tetrafluoropropaneHCID 3765121({4'-Bromo-[1,1'-biphenyl]-4-yl}oxy)(tert-butyl)dimethylsilaneHCID 110762054-Pentyl-4-phenyl-4-silacyclohexanone

생성물 1

HCID 178447728HCID 178447728, 화합물

실험 절차

The general procedure of Example 17 was repeated using 4'-bromo-4-(t-butyldimethylsiloxy)biphenyl, 4-pentyl-4-phenyl-4-silacyclohexanone, and 1-bromo-2,2,3,3-tetrafluoro-n-propane, thereby obtaining the intended compound.

후처리

  1. customobtaining the intended compound

출처 및 근거

ORD 기록
ord-d390d90aa98f4f8d83564c87de726a20
출처 데이터셋
uspto-grants-1999_12
특허 번호
US06004478

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