3-Bromo-1,1,1-trifluoropropane → HCID 178447727, 화합물

HRID 612331

반응식

HRID 612331 반응식
Br[C:2]1[CH:7]=[CH:6][C:5]([C:8]2[CH:13]=[CH:12][C:11]([O:14][Si](C(C)(C)C)(C)C)=[CH:10][CH:9]=2)=[CH:4][CH:3]=1.[CH3:22][CH:23]([CH3:39])[CH2:24][CH2:25][Si:26]1(C2C=CC=CC=2)[CH2:31][CH2:30][C:29](=O)[CH2:28][CH2:27]1.Br[CH2:41][CH2:42][C:43]([F:46])([F:45])[F:44]>>[CH3:39][CH:23]([CH3:22])[CH2:24][CH2:25][Si@H:26]1[CH2:27][CH2:28][C@H:29]([C:2]2[CH:3]=[CH:4][C:5]([C:8]3[CH:9]=[CH:10][C:11]([O:14][CH2:41][CH2:42][C:43]([F:46])([F:45])[F:44])=[CH:12][CH:13]=3)=[CH:6][CH:7]=2)[CH2:30][CH2:31]1

참가 물질

4

반응물 3

HCID 27251143-Bromo-1,1,1-trifluoropropaneHCID 3765121({4'-Bromo-[1,1'-biphenyl]-4-yl}oxy)(tert-butyl)dimethylsilaneHCID 195938624-(3-Methylbutyl)-4-phenyl-4-silacyclohexanone

생성물 1

HCID 178447727HCID 178447727, 화합물

실험 절차

The general procedure of Example 17 was repeated using 4'-bromo-4-(t-butyldimethylsiloxy)biphenyl, 4-(3-methyl-n-butyl)-4-phenyl-4-silacyclohexanone, and 1-bromo-3,3,3-trifluoro-n-propane, thereby obtaining the intended compound.

후처리

  1. customobtaining the intended compound

출처 및 근거

ORD 기록
ord-366bdda7499f4057bc9cbb43877c9f96
출처 데이터셋
uspto-grants-1999_12
특허 번호
US06004478

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