Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Potassium Carbonate → Dimethyl 4-(4-methoxybenzyloxy)phthalate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 반응물 | 4-Methyloxybenzyl chloride | HCID 69993 | — |
| 반응물 | Dimethyl 4-hydroxyphthalate | HCID 89726 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | Dimethyl 4-(4-methoxybenzyloxy)phthalate | HCID 19595683 | — |
반응 단계
1 eq. of dimethyl 4-hydroxyphthalate, 1.1 eq. of potassium carbonate and 1.1 eq. of 4-methoxybenzyl chloride were stirred in DMF at RT. After 4 days, the mixture was worked up according to a standard procedure. Dimethyl 4-(4-methoxybenzyloxy)phthalate was isolated as a colorless oil. MS: 331 ((M+1)+)
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06005010 |
| 출처 데이터셋 | uspto-grants-1999_12 |
| ORD ID | ord-6aa64a686a13461fbdec1ab546ad0f32 |
| 출처 메모 | uspto-grants-1999_12 |