2-Amino-5-methylphenol → HCID 22011341, 화합물

반응식

[OH:1][C:2]1[CH:8]=[C:7]([CH3:9])[CH:6]=[CH:5][C:3]=1[NH2:4].[Br:10][C:11]1[CH:16]=[CH:15][CH:14]=[CH:13][C:12]=1[N:17]=[C:18]=[O:19]>>[OH:1][C:2]1[CH:8]=[C:7]([CH3:9])[CH:6]=[CH:5][C:3]=1[NH:4][C:18]([NH:17][C:12]1[CH:13]=[CH:14][CH:15]=[CH:16][C:11]=1[Br:10])=[O:19]

참가 물질

반응물 2

HCID 760822-Amino-5-methylphenol

HCID 1370972-Bromophenyl isocyanate

생성물 1

HCID 22011341HCID 22011341, 화합물

실험 절차

The urea was prepared from 2-hydroxy 4-methyl aniline (0.274 g, 2 mmol) and 2-bromo phenyl isocyanate (0.40 g, 2 mmol) by general Method B. It was purified by dilution of the DMF solution with methylene chloride and precipitation with hexane (249 mg. 39%) EI-MS m/z 319 (M+)+

후처리

customIt was purified by dilution of the DMF solution with methylene chloride and precipitation with hexane (249 mg. 39%) EI-MS m/z 319

출처 및 근거

ORD 기록: ord-d5b0087d69124dc083adc02f11c3994b
출처 데이터셋: uspto-grants-1999_12
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US06005008

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