Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-Butyn-2-ol → Undec-8-en-3-yne-2,5-diol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-Butyn-2-ol | HCID 16239 | — |
| 반응물 | Hept-4-enal | HCID 71590 | — |
| 반응물 | HCID 178418443 | HCID 178418443 | — |
| 용매 | Tetrahydrofuran | HCID 8028 | — |
| 생성물 | Undec-8-en-3-yne-2,5-diol | HCID 123300045 | — |
반응 단계
But-3-yn-2-ol was added into a solution of ethyl magnesium bromide (EtMgBr) in tetrahydrofuran (THF). Hept-4-enal was then dropped into the mixture at room temperature and aged for 2 hours. The rush over process provided the product undec-8-en-3-yne-2,5-diol.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09441185B2 |
| 출처 데이터셋 | uspto-grants-2016_09 |
| ORD ID | ord-031d4fef6cf0407a9a44ce165221682a |
| 출처 메모 | uspto-grants-2016_09 |