Acetyl chloride → HCID 21329802, 화합물

반응식

[CH3:1][O:2][C:3]1[CH:4]=[C:5]2[O:9][CH:8]([CH3:10])[CH2:7][C:6]2=[C:11]([NH2:13])[CH:12]=1.[C:14](Cl)(=[O:16])[CH3:15].C(OC(C)C)(C)C.C(O)C>>[CH3:1][O:2][C:3]1[CH:12]=[C:11]([NH:13][C:14](=[O:16])[CH3:15])[C:6]2[CH2:7][CH:8]([CH3:10])[O:9][C:5]=2[CH:4]=1

참가 물질

반응물 3

HCID 6367Acetyl chloride

HCID 213298112,3-Dihydro-6-methoxy-2-methyl-4-benzofuranamine

HCID 23358034Diisopropyl ether ethanol

생성물 1

HCID 21329802HCID 21329802, 화합물

실험 절차

This compound is prepared according to the procedures of example 10 by reacting 2,3-dihydro-6-methoxy-2-methyl-4-benzofuranamine with acetyl chloride. M.p. 104° C. (from isopropyl ether/ethyl alcohol).

후처리

customThis compound is prepared

출처 및 근거

ORD 기록: ord-c24975868f554bec9bbe503ee3c32797
출처 데이터셋: uspto-grants-1979_03
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04143055

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