Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
N,N-Dimethyltetradecylamine → HCID 86733511, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | N,N-Dimethyltetradecylamine | HCID 8211 | — |
| 반응물 | Bromomethyl tricyclo[3.3.1.13,7]dec-1-yl ketone | HCID 197820 | — |
| 용매 | Acetone | HCID 180 | — |
| 생성물 | HCID 86733511 | HCID 86733511 | 84.2% |
반응 단계
A mixture of 1.3g. (0.005 mole) 1-adamantyl bromomethyl ketone and 1.23g (0.005 mole) dimethyltetradecylamine was solubilized by the addition of 30cc acetone. The next day the solidified mixture was washed with ether and recrystallized from ethyl acetate to yield 2.1g white crystals, m.p. 134°-135.5°.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04143127 |
| 출처 데이터셋 | uspto-grants-1979_03 |
| ORD ID | ord-7f8144f1ac4a41dd89582865bff2707e |
| 출처 메모 | uspto-grants-1979_03 |