Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 614424생성일: 2026년 10월 27일
Sodium Trithiocarbonate → Sodium (2-methyl-3-hydroxy-5-vinyl-4-pyridinyl)methyl trithiocarbonate
https://huagongshe.com/reaction/614424
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Sodium Trithiocarbonate | HCID 101753 | — |
| 반응물 | 2-Methyl-3-hydroxy-4-chloromethyl-5-vinylpyridine | HCID 20263960 | — |
| 용매 | Methanol--water (1/1) | HCID 22242641 | — |
| 생성물 | Sodium (2-methyl-3-hydroxy-5-vinyl-4-pyridinyl)methyl trithiocarbonate | HCID 86736400 | — |
반응 단계
2-Methyl-3-hydroxy-4-chloromethyl-5-vinylpyridine (20 g.) is suspended in water/methanol (100:25 v/v) and treated with disodium trithiocarbonate (33%) (45 g.). The mixture is stirred at b 50° C. for 4 hours under nitrogen and adjusted to pH 6.2-6.5 with dilute acid. The precipitate is recrystallized from DMF/water to give sodium (2-methyl-3-hydroxy-5-vinyl-4-pyridinyl)methyl trithiocarbonate.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 특허 번호 | US04144342 |
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| 출처 데이터셋 | uspto-grants-1979_03 |
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| ORD ID | ord-0a0bd7c9e6a84b43aa484dc988503ae7 |
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| 출처 메모 | uspto-grants-1979_03 |
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