Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethyl 2-oxopyrrolidine-1-acetate → (+/-)-N-[2-(4-methyl-1-piperazinyl)propyl]-2-oxo-1-pyrrolidineacetamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethyl 2-oxopyrrolidine-1-acetate | HCID 109094 | — |
| 반응물 | 2-(4-Methylpiperazin-1-yl)propan-1-amine | HCID 16641457 | — |
| 생성물 | (+/-)-N-[2-(4-methyl-1-piperazinyl)propyl]-2-oxo-1-pyrrolidineacetamide | HCID 21327809 | — |
반응 단계
From 7.0 g. of ethyl 2-oxo-1-pyrrolidineacetate and 6.3 g. of 2-(4-methyl-1-piperazinyl)propylamine, following the procedure of Example 9, there is obtained (±)-N-[2-(4-methyl-1-piperazinyl)propyl]-2-oxo-1-pyrrolidineacetamide; m.p. 84°-85° C. after recrystallization from cyclohexane and from heptane.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04145347 |
| 출처 데이터셋 | uspto-grants-1979_03 |
| ORD ID | ord-1d6feda2a2f540c69ff66a6f425f5c7a |
| 출처 메모 | uspto-grants-1979_03 |