Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1,2-Ethanediamine, N1,N1-bis(1-methylethyl)- → N-[2-[Bis(1-methylethyl)amino]ethyl]-2-methyl-5-oxo-1-pyrrolidineacetamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1,2-Ethanediamine, N1,N1-bis(1-methylethyl)- | HCID 8459 | — |
| 반응물 | 1-Pyrrolidineacetic acid, 2-methyl-5-oxo-, ethyl ester | HCID 574476 | — |
| 생성물 | N-[2-[Bis(1-methylethyl)amino]ethyl]-2-methyl-5-oxo-1-pyrrolidineacetamide | HCID 44374465 | — |
반응 단계
From 9.2 g. of ethyl 2-methyl-5-oxo-1-pyrrolidineacetate and 8.7 g. of 2-(diisopropylamino)ethylamine, following the procedure of Example 9, there is obtained N-[2-[Bis(1-methylethyl)amino]ethyl]-2-methyl-5-oxo-1-pyrrolidineacetamide; m.p. 73°-74° C. after recrystallization from hexane.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04145347 |
| 출처 데이터셋 | uspto-grants-1979_03 |
| ORD ID | ord-4243bfd66dba4307827fc3fb5f394bb3 |
| 출처 메모 | uspto-grants-1979_03 |