2-Methoxy-5-Methylaniline → HCID 86734248, 화합물

HRID 614735

반응식

HRID 614735 반응식
[Cl-:1].[CH3:2][N+:3]([CH3:20])([CH2:10][C:11]1[CH:16]=[CH:15][C:14]([O:17][CH3:18])=[C:13]([NH2:19])[CH:12]=1)[CH2:4][CH2:5][CH2:6][NH:7]C=O.[Cl-].C[N+](C)([CH2:28][C:29]1[CH:34]=[CH:33][C:32]([O:35][CH3:36])=[C:31]([NH2:37])[CH:30]=1)CCCN.[NH2:39]C1C=C(C)C=CC=1OC>>[Cl-:1].[CH3:20][N+:3]([CH3:2])([CH2:10][C:11]1[CH:16]=[CH:15][C:14]([O:17][CH3:18])=[C:13]([N:19]=[N:39][C:34]2[CH:33]=[C:32]([O:35][CH3:36])[C:31]([NH2:37])=[CH:30][C:29]=2[CH3:28])[CH:12]=1)[CH2:4][CH2:5][CH2:6][NH2:7]

참가 물질

4

반응물 3

HCID 84452-Methoxy-5-MethylanilineHCID 86734246HCID 86734246, 화합물HCID 86734247HCID 86734247, 화합물

생성물 1

HCID 86734248HCID 86734248, 화합물

실험 절차

Proceeding in a manner similar to that described above in Example 3, N,N-dimethyl-N-(3-amino-4-methoxybenzyl)-N-3-formamidopropylammonium chloride was hydrolyzed and the resulting N,N-dimethyl-N-(3-amino-4-methoxybenzyl)-N-3-aminopropylammonium chloride was diazotized and coupled with 2-amino-4-methylanisole to obtain N,N-dimethyl-N-[3-(4-amino-5-methoxy-2-methylphenyl)azo-4-methoxybenzyl]-N-3-aminopropylammonium chloride in aqueous solution. This product was diazotized in situ and coupled with acetoacetanilide to obtain the brown, water-soluble dyestuff having the formula ##STR100##

출처 및 근거

ORD 기록
ord-f30bfa40cacf4c819f4a9cad6d97e16b
출처 데이터셋
uspto-grants-1979_03
특허 번호
US04146558

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