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Methyl chloroformate → Methyl [1-(3-nitrophenyl)propan-2-yl]carbamate

HRID 614877
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HRID 614877 반응식
Cl[C:2]([O:4][CH3:5])=[O:3].[N+:6]([C:9]1[CH:10]=[C:11]([CH2:15][CH:16]([NH2:18])[CH3:17])[CH:12]=[CH:13][CH:14]=1)([O-:8])=[O:7].C(=O)([O-])[O-].[K+].[K+]>C(#N)C>[N+:6]([C:9]1[CH:10]=[C:11]([CH2:15][CH:16]([NH:18][C:2]([O:4][CH3:5])=[O:3])[CH3:17])[CH:12]=[CH:13][CH:14]=1)([O-:8])=[O:7]
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참가 물질

5

반응물 3

HCID 6586Methyl chloroformateHCID 11430Potassium CarbonateHCID 19783051HCID 19783051, 화합물

생성물 1

HCID 21327418Methyl [1-(3-nitrophenyl)propan-2-yl]carbamate

시약·촉매·용매 1

HCID 6342Acetonitrile용매

실험 절차

5.33 ml of methyl chloroformate were added dropwise to a mixture consisting of 12.6 gm of 1-(3'-nitro-phenyl)-2-amino-propane, 9.8 gm of potassium carbonate and 100 ml of acetonitrile, whereby the temperature of the mixture rose to 45° C., and the resulting mixture was boiled for two hours. Thereafter, the reaction mixture was diluted with ice water, and the crystals precipitated thereby were collected by suction filtration, washed with water and dried, yielding 11 gm of 1-(3'-nitro-phenyl)-2-(methoxycarbonyl-amino)-propane, m.p. 104°-105° C. This compound was hydrogenated in methanol in the presence of Raney nicket at atmospheric pressure and room temperature. Thereafter, the catalyst was removed by suction filtration, the methanol was distilled out of the filtrate, and the residue, 1-(3'-amino-phenyl)-2-(methoxycarbonyl-amino)-propane, was dissolved in acetonitrile. The resulting solution was admixed with the calculated amount of maleic acid, and the precipitate formed thereby was recrystallized twice from acetonitrile, yielding 5.5 gm of the maleate of the formual ##STR27## which had a melting point of 125°-127° C.

후처리

  1. customrose to 45° C.
  2. customthe crystals precipitated
  3. filtrationthereby were collected by suction filtration
  4. washwashed with water
  5. customdried

출처 및 근거

ORD 기록
ord-76a44552093a463884a83d33c288598f
출처 데이터셋
uspto-grants-1979_03
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US04146645

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