Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Glyceraldehyde → 4-(n-Hexadecylamino)benzoyl glyceraldehyde
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Glyceraldehyde | HCID 751 | — |
| 반응물 | Chloroform | HCID 6212 | — |
| 반응물 | 4-Hexadecylaminobenzoyl chloride hydrochloride | HCID 13255322 | — |
| 촉매 | 4-(Dimethylamino)pyridine | HCID 14284 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | 4-(n-Hexadecylamino)benzoyl glyceraldehyde | HCID 21326953 | — |
반응 단계
To a mixture of 3.6 g. of glyceraldehyde and 2.44 g. of 4-dimethylaminopyridine in an ice-bath is added 4.16 g. of 4-(n-hexadecylamino)benzoyl chloride hydrochloride. After 4 hours at room temperature, chloroform and water are added. The chloroform extract is chromatographed quickly and evaporated in vacuo to yield 4-(n-hexadecylamino)benzoyl glyceraldehyde.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04146546 |
| 출처 데이터셋 | uspto-grants-1979_03 |
| ORD ID | ord-66fef1a1db6948c9940bcde96e59a27b |
| 출처 메모 | uspto-grants-1979_03 |