Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sodium Hydroxide → Robinin silver
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | Silver | HCID 23954 | — |
| 반응물 | Robinin | HCID 5281693 | — |
| 용매 | Water | HCID 962 | — |
| 용매 | Benzenesulfonic acid, 4-methyl-, silver(1+) salt (1:1) | HCID 85606 | — |
| 생성물 | Robinin silver | HCID 131737180 | — |
반응 단계
Robinin/silver colloidal nanoparticle catalyst is prepared by dissolving 1.07 g robinin in a beaker containing 800 ml DI water at room temperature. 1 N NaOH solution is added with stirring to adjust the solution pH to 11. In a separate beaker, 1.42 g silver p-toluenesulfonate is dissolved in 40 ml DI water. The silver ion solution is added to the robinin solution with vigorous stirring. The molar ratio of silver metal to robinin is 1:0.28. The beaker containing the aqueous catalyst solution is placed in a 50° C. water bath for 12 hours to test its stability. After 12 hours the solution is observed and no precipitate is expected indicating that the catalyst is still stable.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09441300B2 |
| 출처 데이터셋 | uspto-grants-2016_09 |
| ORD ID | ord-64150bcd57e847049c37bcfb81e28339 |
| 출처 메모 | uspto-grants-2016_09 |