Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetone → 7,8-Dichloro-1,2-dihydro-2,2,3-trimethyl-1,3,5-triazino[1,2-a]benzimidazol-4(3H)-one
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetone | HCID 180 | — |
| 반응물 | Methyl Isocyanate | HCID 12228 | — |
| 반응물 | 2-Amino-5,6-dichlorobenzimidazole | HCID 466016 | — |
| 생성물 | 7,8-Dichloro-1,2-dihydro-2,2,3-trimethyl-1,3,5-triazino[1,2-a]benzimidazol-4(3H)-one | HCID 135797529 | — |
반응 단계
Reaction of 2-amino-5,6-dichlorobenzimidazole with acetone and methyl isocyanate according to the procedure of Example 1, first paragraph, provided the title compound. In this case, a 10-N-methylcarbamoyl derivative was not isolated from the reaction mixture. The product was recrystallized from acetone to give a solid, mp 220° C. (dec.). The confirmatory elemental analysis is shown in Table III.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04498920 |
| 출처 데이터셋 | uspto-grants-1985_02 |
| ORD ID | ord-99e8f81173784a4e8d0d12ff3f86fd1d |
| 출처 메모 | uspto-grants-1985_02 |