Aniline → HCID 20427456, 화합물

HRID 615307

반응식

HRID 615307 반응식
[OH:1][C:2]1[CH:11]=[CH:10][C:9]([OH:12])=[C:8]2[C:3]=1[C:4](=[O:14])[CH:5]=[CH:6][C:7]2=[O:13].[NH2:15][C:16]1[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1>C(O)C>[NH:15]([C:10]1[C:9](=[O:12])[C:8]2[C:3]([C:2](=[O:1])[CH:11]=1)=[C:4]([OH:14])[C:5]([NH:15][C:16]1[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1)=[CH:6][C:7]=2[OH:13])[C:16]1[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1

참가 물질

4

반응물 2

HCID 6115AnilineHCID 10141Naphthazarin

생성물 1

HCID 20427456HCID 20427456, 화합물

시약·촉매·용매 1

HCID 702Ethanol용매

실험 절차

A mixture of 1.9 g of 5,8-dihydroxy-1,4-naphthoquinone and 40 ml of aniline is heated at 100° for 8 hours. After the mixture has been cooled and diluted with ethanol, 2,6-bis-anilino-5,8-dihydroxy-1,4-naphthoquinone is obtained.

후처리

  1. temperatureis heated at 100° for 8 hours
  2. temperatureAfter the mixture has been cooled

출처 및 근거

ORD 기록
ord-cd764ba17f10422da02f36478fd83005
출처 데이터셋
uspto-grants-1985_02
특허 번호
US04499004

연결된 노트

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