Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrochloric Acid → Acetylphenylstearic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | Acetyl chloride | HCID 6367 | — |
| 반응물 | Aluminum(III) Chloride | HCID 6451240 | — |
| 반응물 | 2-Phenyloctadecanoic acid | HCID 22015237 | — |
| 반응물 | HCID 131714100 | HCID 131714100 | — |
| 용매 | Carbon Tetrachloride | HCID 5943 | — |
| 생성물 | Acetylphenylstearic acid | HCID 70477797 | — |
반응 단계
A 500 ml reaction vessel was charged with 200 mls freshly distilled carbon tetrachloride and the CCl4 was cooled to 0°-5° C. Aluminum chloride (0.33 moles) was added, via Gooch tubing, to the CCl4 over a period of 20 minutes. Acetyl chloride (0.35 mol) was added to an addition funnel and charged to the CCl4 -AlCl3 mixture. Phenylstearic acid (0.125 moles) was then slowly added to the reaction mixture from an addition funnel while maintaining the temperature of the reaction mixture at 0°-5° C. The temperature was maintained at 0°-5° C. for one hour and at room temperature for an additional two hours. The evolution of HCl was observed.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04499013 |
| 출처 데이터셋 | uspto-grants-1985_02 |
| ORD ID | ord-81c1187f66ae4a17949542ab91d3be67 |
| 출처 메모 | uspto-grants-1985_02 |