Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Diisopropylamine → HCID 13272378, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Diisopropylamine | HCID 7912 | — |
| 반응물 | Ethyl chloroformate | HCID 10928 | — |
| 반응물 | 3-Isoquinolinecarboxylicacid, 1-(2-chlorophenyl)- | HCID 11000554 | — |
| 용매 | Triethylamine | HCID 8471 | — |
| 생성물 | HCID 13272378 | HCID 13272378 | 23.2% |
반응 단계
Operations are carried out as for Example 7, starting from 2.83 g of 1-(2-chloro phenyl) isoquinoline 3-carboxylic acid, 1.17 g of triethylamine, 1.25 g of ethyl chloroformate and 1.31 g of di-isopropylamine in 100 ml of chlorofom. 0.85 g of N,N-di(1-methyl ethyl) 1-(2-chloro phenyl) isoquinoline 3-carboxamide, melting at 161° C., is obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04499094 |
| 출처 데이터셋 | uspto-grants-1985_02 |
| ORD ID | ord-782300f7520f40ef882ecfdb198c7fef |
| 출처 메모 | uspto-grants-1985_02 |