Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Diethylene Glycol Monoethyl Ether → Ethylene brassylate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Diethylene Glycol Monoethyl Ether | HCID 8146 | — |
| 반응물 | Sodium Stearate | HCID 2724691 | — |
| 반응물 | Potassium Stearate | HCID 23673840 | — |
| 생성물 | Ethylene brassylate | HCID 61014 | 73.2% |
반응 단계
Repeating Example X, a double metal salt was prepared except that sodium stearate was substituted for the potassium stearate and the ethyl cellusolve was replaced with diethylene glycol monoethyl ether. The resulting double metal salt NaAl(OC2H4OC2H4OC2H5)3 (OOCC17H35) was used as the catalyst for the continuous depolymerization of poly(ethylene brassylate) in accordance with the procedure and conditions of Example I. Ethylene brassylate was continuously produced and distilled from the reactor at a rapid rate and the overall yield was 73.2 percent. Comparable results are obtained using the double metal salt NaAl(OC2H4OC2H5)3 (OOCC6H5) obtained by the reaction of sodium benzoate and aluminum tricellusolve (Al(OC2H4OC2H5)3).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04499288 |
| 출처 데이터셋 | uspto-grants-1985_02 |
| ORD ID | ord-2d033621c2744873a01ccbf60615cd26 |
| 출처 메모 | uspto-grants-1985_02 |