Epichlorohydrin → 7-(2,3-Epoxypropoxy)-3-phenylchromone

HRID 615880

반응식

HRID 615880 반응식
[OH:1][C:2]1[CH:11]=[C:10]2[C:5]([C:6](=[O:18])[C:7]([C:12]3[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=3)=[CH:8][O:9]2)=[CH:4][CH:3]=1.[CH2:19]([CH:21]1[O:23][CH2:22]1)Cl>C(O)(C)C>[O:23]1[CH2:22][CH:21]1[CH2:19][O:1][C:2]1[CH:11]=[C:10]2[C:5]([C:6](=[O:18])[C:7]([C:12]3[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=3)=[CH:8][O:9]2)=[CH:4][CH:3]=1

참가 물질

4

반응물 2

HCID 7835EpichlorohydrinHCID 53768917-Hydroxyisoflavone

생성물 1

HCID 101084827-(2,3-Epoxypropoxy)-3-phenylchromone

시약·촉매·용매 1

HCID 3776Isopropanol용매

실험 절차

7-Hydroxy-3-phenylchromone and epichlorohydrin were reacted according to general procedure A, and the product obtained was white prisms, m.p. 151°-152° (83% crude yield) from isopropyl alcohol.

후처리

  1. customthe product obtained

출처 및 근거

ORD 기록
ord-370c501dd66346c7bd132900c8cb11cd
출처 데이터셋
uspto-grants-1985_02
특허 번호
US04501755

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