Propanamide, 2-chloro-N,N-dimethyl- → HCID 20308970, 화합물

반응식

[CH3:1][C:2]1[C:3]([C:7]2[CH:12]=[CH:11][CH:10]=CC=2)=[N:4][NH:5][CH:6]=1.Br[CH:14]([CH2:20][CH2:21][CH3:22])[C:15]([N:17]([CH3:19])[CH3:18])=[O:16].ClC(C)C(N(C)C)=[O:26]>>[O:26]1[CH:10]=[CH:11][CH:12]=[C:7]1[C:3]1[C:2]([CH3:1])=[CH:6][N:5]([CH:14]([CH2:20][CH2:21][CH3:22])[C:15]([N:17]([CH3:19])[CH3:18])=[O:16])[N:4]=1

참가 물질

반응물 3

HCID 112034Propanamide, 2-chloro-N,N-dimethyl-

HCID 19856204HCID 19856204, 화합물

HCID 178430907HCID 178430907, 화합물

생성물 1

HCID 20308970HCID 20308970, 화합물

실험 절차

Following the procedure of Example 1, but substituting 3-(2-furyl)-4-methylpyrazole for 4-methyl-3-phenylpyrazole and 2-bromo-N,N-dimethylvaleramide for 2-chloro-N,N-dimethylpropionamide there was obtained 3-(2-furyl)-N,N,4-trimethyl-α-propylpyrazole-1-acetamide having a melting point of 107°-109° C.

출처 및 근거

ORD 기록: ord-da1a0125cef14d6cacd35a1ac68442e1
출처 데이터셋: uspto-grants-1978_02
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04072498

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