Propanamide, 2-chloro-N,N-dimethyl- → HCID 20370560, 화합물

반응식

[CH3:1][C:2]1[C:3]([C:7]2[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=2)=[N:4][NH:5][CH:6]=1.Br[CH:14]([CH2:20][CH3:21])[C:15]([N:17]([CH3:19])[CH3:18])=[O:16].[Cl:22]C(C)C(N(C)C)=O>>[Cl:22][C:12]1[CH:11]=[CH:10][CH:9]=[CH:8][C:7]=1[C:3]1[C:2]([CH3:1])=[CH:6][N:5]([CH:14]([CH2:20][CH3:21])[C:15]([N:17]([CH3:19])[CH3:18])=[O:16])[N:4]=1

참가 물질

반응물 3

HCID 112034Propanamide, 2-chloro-N,N-dimethyl-

HCID 30160612-Bromo-N,N-dimethylbutanamide

HCID 178430907HCID 178430907, 화합물

생성물 1

HCID 20370560HCID 20370560, 화합물

실험 절차

Following the procedure of Example 1, but substituting 3-(o-chlorophenyl)-4-methylpyrazole for 4-methyl-3-phenylpyrazole and 2-bromo-N,N-dimethylbutyramide for 2-chloro-N,N-dimethylpropionamide there was obtained 3-(o-chlorophenyl)-α-ethyl-N,N,4-trimethylpyrazole-1-acetamide having a boiling point of 180°/0.15 mm.

출처 및 근거

ORD 기록: ord-729db3861a994c868ed2724afee2840f
출처 데이터셋: uspto-grants-1978_02
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04072498

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