Ammonia → HCID 20370606, 화합물

HRID 615969노트

반응식

HRID 615969 반응식
[CH3:1][CH:2]([N:6]1[CH:10]=[C:9](C)[C:8]([C:12]2[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=2)=[N:7]1)[C:3]([OH:5])=O.[CH2:18]([NH:20][CH2:21][CH3:22])[CH3:19].N>>[CH2:18]([N:20]([CH2:21][CH3:22])[C:3](=[O:5])[CH:2]([CH3:1])[N:6]1[CH:10]=[CH:9][C:8]([C:12]2[CH:13]=[CH:14][CH:15]=[CH:16][CH:17]=2)=[N:7]1)[CH3:19]

참가 물질

4

반응물 3

HCID 222AmmoniaHCID 8021DiethylamineHCID 20370468alpha,4-Dimethyl-3-phenyl-1H-pyrazole-1-acetic acid

생성물 1

HCID 20370606HCID 20370606, 화합물

실험 절차

Following the procedure of Example 68, but substituting α-methyl-3-phenylpyrazole-1-acetic acid for α,4-dimethyl-3-phenylpyrazole-1-acetic acid, and diethylamine for aqueous ammonia there was obtained N,N-diethyl-α-methyl-3-phenylpyrazole-1-acetamide having a boiling point of 178°/0.2 mm.

출처 및 근거

ORD 기록
ord-d787b9600f754e28a114c80ad8925609
출처 데이터셋
uspto-grants-1978_02
특허 번호
US04072498

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