Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methoxycarbonyl isothiocyanate → 1-(3-Methoxycarbonyl-2-thioureido)-5-methylthio-2-nitrobenzene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methoxycarbonyl isothiocyanate | HCID 552246 | — |
| 반응물 | 5-(Methylthio)-2-nitroaniline | HCID 10535482 | — |
| 용매 | Acetone | HCID 180 | — |
| 생성물 | 1-(3-Methoxycarbonyl-2-thioureido)-5-methylthio-2-nitrobenzene | HCID 20371013 | — |
반응 단계
1.5 G. 2-amino-4-methylthio-1-nitrobenzene in 30 ml. acetone is treated with 2.5 g. methoxy carbonyl isothiocyanate. After five days the mixture is stripped under vacuum and the residue triturated with methanol yielding 1-(3-methoxycarbonyl-2-thioureido)-5-methylthio-2-nitrobenzene.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04072696 |
| 출처 데이터셋 | uspto-grants-1978_02 |
| ORD ID | ord-e2419b17992a4f959a0d94d29c9744de |
| 출처 메모 | uspto-grants-1978_02 |