Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetonitrile → Disodium adipate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetonitrile | HCID 6342 | — |
| 반응물 | Dimethyladipate | HCID 12329 | — |
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | Disodium adipate | HCID 24073 | — |
반응 단계
17.4 Grams (0.1 mole) of dimethyl adipate are dissolved in 100 mls. of acetonitrile and heated to 70° C. 8.2 Grams (0.2 mole) of sodium hydroxide dissolved in 6.0 g. of water are added to the reaction mixture. The reaction mixture is stirred at reflux temperature for 18 hours. The resulting solution is filtered hot and the solids are air dried to yield disodium adipate as the reaction product.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04075234 |
| 출처 데이터셋 | uspto-grants-1978_02 |
| ORD ID | ord-4a44ab5cc5df4d7eaf36af8930e8ae52 |
| 출처 메모 | uspto-grants-1978_02 |