Acetonitrile → Disodium adipate

HRID 616621

반응식

HRID 616621 반응식
[C:1]([O:11]C)(=[O:10])[CH2:2][CH2:3][CH2:4][CH2:5][C:6]([O:8]C)=[O:7].C(#N)C.[OH-].[Na+:17]>O>[C:1]([O-:11])(=[O:10])[CH2:2][CH2:3][CH2:4][CH2:5][C:6]([O-:8])=[O:7].[Na+:17].[Na+:17]

참가 물질

5

반응물 3

HCID 6342AcetonitrileHCID 12329DimethyladipateHCID 14798Sodium Hydroxide

생성물 1

HCID 24073Disodium adipate

시약·촉매·용매 1

HCID 962Water용매

실험 절차

17.4 Grams (0.1 mole) of dimethyl adipate are dissolved in 100 mls. of acetonitrile and heated to 70° C. 8.2 Grams (0.2 mole) of sodium hydroxide dissolved in 6.0 g. of water are added to the reaction mixture. The reaction mixture is stirred at reflux temperature for 18 hours. The resulting solution is filtered hot and the solids are air dried to yield disodium adipate as the reaction product.

후처리

  1. temperatureat reflux temperature for 18 hours
  2. filtrationThe resulting solution is filtered hot
  3. customdried

출처 및 근거

ORD 기록
ord-4a44ab5cc5df4d7eaf36af8930e8ae52
출처 데이터셋
uspto-grants-1978_02
특허 번호
US04075234

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