Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrogen Bromide → Silver bromide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrogen Bromide | HCID 260 | — |
| 반응물 | Lauric Acid | HCID 3893 | — |
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | Silver Nitrate | HCID 24470 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | Silver bromide | HCID 66199 | — |
| 생성물 | Silver laurate | HCID 9904644 | — |
반응 단계
One liter of an aqueous solution of 20 g of sodium hydroxide was mixed with 2 liters of toluene having dissolved therein 120 g of lauric acid, and the mixture was emulsified using a high speed rotary stirrer. To the emulsion, 500 ml of a 0.4% by weight aqueous solution of hydrobromic acid was added, and the mixture was again emulsified. To the resulting emulsion, 500 ml of an aqueous solution of 85 g of silver nitrate was added to form silver laurate and silver bromide simultaneously. The toluene phase containing the silver nitrate and the silver bromide was separated from the aqueous phase, and dispersed in 2.4 Kg of a 15% by weight isopropanol solution of polyvinyl butyral using a high speed rotary stirrer.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04076534 |
| 출처 데이터셋 | uspto-grants-1978_02 |
| ORD ID | ord-295ec46675b645f9b71b64ae2c3039dd |
| 출처 메모 | uspto-grants-1978_02 |