참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Phosgene | HCID 6371 | — |
| 반응물 | 10-fluoro-5H-dibenz[b,f]azepine | HCID 20366408 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | 10-fluoro-5H-dibenz[b,f]azepine-5-carbonyl chloride | HCID 20366410 | — |
반응 단계
A mixture of 2.3 g of 10-fluoro-5H-dibenz[b,f]azepine and 30 ml of toluene saturated with phosgene is stirred for 2 days at 25° C. Excess phosgene is then expelled with nitrogen and the reaction mixture is concentrated by rotary evaporation to yield crude 10-fluoro-5H-dibenz[b,f]azepine-5-carbonyl chloride as residue.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04076812 |
|---|
| 출처 데이터셋 | uspto-grants-1978_02 |
|---|
| ORD ID | ord-84342a3214e94d54b38ef2410a598ec3 |
|---|
| 출처 메모 | uspto-grants-1978_02 |
|---|
