beta-Aminobeta-ethoxyacrylic acid ethyl ester → HCID 20367323, 화합물

반응식

C([O:3][C:4](=O)[CH:5]=[C:6]([NH2:10])OCC)C.[Cl:12][C:13]1[CH:21]=[CH:20][CH:19]=[C:18]([Cl:22])[C:14]=1[CH2:15][NH:16][NH2:17]>>[NH2:10][C:6]1[NH:17][N:16]([CH2:15][C:14]2[C:13]([Cl:12])=[CH:21][CH:20]=[CH:19][C:18]=2[Cl:22])[C:4](=[O:3])[CH:5]=1

참가 물질

반응물 2

HCID 278451beta-Aminobeta-ethoxyacrylic acid ethyl ester

HCID 46250371-(2,6-Dichlorobenzyl)hydrazine

생성물 1

HCID 20367323HCID 20367323, 화합물

실험 절차

35 g of β-amino-β-ethoxyacrylic acid ethyl ester and 38 g of 2,6-dichlorobenzylhydrazine when reacted as described in Example 45, yield 24 g of the compound identified above as colorless crystals, corresponding to 46% of theory, of melting point 225°.

출처 및 근거

ORD 기록: ord-3cb2f1c3532449e18ef2d3d174693871
출처 데이터셋: uspto-grants-1978_02
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04076943

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