참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Nitric Acid | HCID 944 | — |
| 반응물 | N-(2,4-Dimethylphenyl)acetamide | HCID 16303 | — |
| 용매 | Sulfuric Acid | HCID 1118 | — |
| 생성물 | Acetamide, N-(2,4-dimethyl-5-nitrophenyl)- | HCID 112848 | — |
반응 단계
A mixture of concentrated nitric acid (20 mL) and concentrated sulfuric acid (20 mL) was cooled in an ice-salt bath to 0° C. N-(2,4-dimethylphenyl)acetamide (9.5 g) was added portionwise at such a rate to maintain the temperature below 5° C. The mixture was then allowed to stir in the cold for an additional one hour.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US05952362 |
|---|
| 출처 데이터셋 | uspto-grants-1999_09 |
|---|
| ORD ID | ord-80511f65a2bb47f180d0bd088cb65e37 |
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| 출처 메모 | uspto-grants-1999_09 |
|---|
