Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-Iodohexane → Methyl 2-hydroxy-4-[7-(1-adamantyl)-6-hexyloxy-2-naphthyl]benzoate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-Iodohexane | HCID 12527 | — |
| 반응물 | Methyl 2-hydroxy-4-[7-(1-adamantyl)-6-hydroxy-2-naphthyl]benzoate | HCID 22000320 | — |
| 생성물 | Methyl 2-hydroxy-4-[7-(1-adamantyl)-6-hexyloxy-2-naphthyl]benzoate | HCID 22000297 | 55% |
반응 단계
Following the procedure of Example 1(a), but reacting 430 mg (1 mmol) of methyl 2-hydroxy-4-[7-(1-adamantyl)-6-hydroxy-2-naphthyl]benzoate with 180 μl (1.2 mmol) of 6-iodohexane, 280 mg (55%) of methyl 2-hydroxy-4-[7-(1-adamantyl)-6-hexyloxy-2-naphthyl]benzoate were obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05952382 |
| 출처 데이터셋 | uspto-grants-1999_09 |
| ORD ID | ord-4c1e3c9840214f13b9f2df01de932ffa |
| 출처 메모 | uspto-grants-1999_09 |