Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methyl 5-bromothiophene-2-carboxylate → HCID 22000374, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methyl 5-bromothiophene-2-carboxylate | HCID 605713 | — |
| 반응물 | 7-(1-Adamantyl)-6-benzyloxy-2-naphthylboronic acid | HCID 22000313 | — |
| 생성물 | HCID 22000374 | HCID 22000374 | 65.5% |
반응 단계
Following the procedure of Example 1(c), but reacting 1.5 g (3.6 mmol) of 7-(l-adamantyl)-6-benzyloxy-2-naphthylboronic acid with 400 mg (1.8 mmol) of methyl 5-bromo-2-thiophenecarboxylate, 600 mg (65%) of the expected compound were obtained, which compound had a melting point of 170°-1° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05952382 |
| 출처 데이터셋 | uspto-grants-1999_09 |
| ORD ID | ord-04286c2faeac4fcbae01bd8dac08d730 |
| 출처 메모 | uspto-grants-1999_09 |