Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Salicylic Acid → HCID 178455906, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Salicylic Acid | HCID 338 | — |
| 반응물 | CID 86674079 | HCID 86674079 | — |
| 용매 | Acetonitrile--water (1/1) | HCID 18373917 | — |
| 생성물 | HCID 178455906 | HCID 178455906 | — |
반응 단계
Salicylic acid (138.12 g/mol, 0.15 mg) 1.5 mg salicylic acid was dissolved in 100 μl ACN/H2O 50/50 mixture to give the mother solution. 10 μl of this latter solution were then added to 0.76 mg exendin-4 acetate dissolved in 50 μl ACN/H2O 50/50 followed by speedvac 2×1 hour as above at approximately 35° C., affording exendin-4 salicylate as a white solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09445992B2 |
| 출처 데이터셋 | uspto-grants-2016_09 |
| ORD ID | ord-a82eea5de7aa439dba4c27bf304e8613 |
| 출처 메모 | uspto-grants-2016_09 |