홈MCP워크벤치Skills
홈워크벤치알림마이페이지
llms.txt · MCP 가이드개인정보처리방침 · 이용약관 · 지원v1.8.0
  1. 홈
  2. /반응

Butyl isocyanate → Urea, N,N-diphenyl-N'-butyl-

HRID 620472
노트
인쇄 미리보기

반응식

HRID 620472 반응식
[C:1]1([NH:7][C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH2:14]([N:18]=[C:19]=[O:20])[CH2:15][CH2:16][CH3:17]>C1(C)C(C)=CC=CC=1.P([O-])(OCCCC)(OCCCC)=O>[CH2:14]([NH:18][C:19]([N:7]([C:1]1[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1)[C:8]1[CH:9]=[CH:10][CH:11]=[CH:12][CH:13]=1)=[O:20])[CH2:15][CH2:16][CH3:17]
참가 물질반응 조건실험 절차후처리출처 및 근거반응 노트

참가 물질

5

반응물 2

HCID 8110Butyl isocyanateHCID 11487Diphenylamine

생성물 1

HCID 14204127Urea, N,N-diphenyl-N'-butyl-수율 60%

시약·촉매·용매 2

HCID 3790919Dibutyl phosphate anion촉매HCID 7237O-Xylene용매

반응 조건

온도
120 °C

실험 절차

0.5 mole of diphenylamine was taken together with 0.53 mole of n-butyl isocyanate and 1 g of di-n-butyl phosphate in 150 ml of xylene. The mixture was heated at 120° C. for 24 hours, with stirring, and then cooled to room temperature. After the product had been filtered off, washed with 100 ml of cold xylene and dried, 0.3 mole of N-n-butyl-N',N'-diphenylurea was obtained. Melting point: 92° C./yield: 60% of theory.

후처리

  1. temperaturecooled to room temperature
  2. filtrationAfter the product had been filtered off
  3. washwashed with 100 ml of cold xylene
  4. customdried

출처 및 근거

ORD 기록
ord-0866a8e646a24c0499f049e1d4316866
출처 데이터셋
uspto-grants-1989_04
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US04820871

반응 노트

불러오는 중…

이 페이지에서참가 물질반응 조건실험 절차후처리출처 및 근거반응 노트