Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-Pyrenecarboxaldehyde → 2-Isopropyl-2-((1-pyrenylmethyl)amino)-1,3-propanediol hydrochloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-Pyrenecarboxaldehyde | HCID 232848 | — |
| 반응물 | 2-Amino-2-isopropyl-1,3-propanediol acetate | HCID 14391248 | — |
| 반응물 | (+-)(2R*,3S*)-2-((1-Pyrenylmethyl)amino)-2-methyl-1,3-butanediol hydrochloride | HCID 86742932 | — |
| 생성물 | 2-Isopropyl-2-((1-pyrenylmethyl)amino)-1,3-propanediol hydrochloride | HCID 21247340 | — |
반응 단계
Using the reductive amination procedure described for 20G, pyrene-1-carbaldehyde (Aldrich) and 2-amino-2-isopropyl-1,3-propanediol acetate (24B) gave 2-isopropyl-2-((1-pyrenylmethyl)amino)-1,3-propanediol hydrochloride mp 244°-245° (dec), (CH3OH/Et2O), (C, H, N, Cl).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04820873 |
| 출처 데이터셋 | uspto-grants-1989_04 |
| ORD ID | ord-306addfc3f9645b6b26bd46dbb57a372 |
| 출처 메모 | uspto-grants-1989_04 |