참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Dimethylformamide | HCID 6228 | — |
| 반응물 | 3-Nitrophenol | HCID 11137 | — |
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 반응물 | Tetradecanoic acid, 2-bromo-, ethyl ester | HCID 85791 | — |
| 용매 | Acetic Acid | HCID 176 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | Ethyl 2-(3-nitrophenoxy)tetradecanoate | HCID 14122414 | — |
반응 단계
A mixture of 250 g (1.79 mol) of m-nitrophenol, 602 g (1.79 mol) of Alphabromo-myristic acid ethyl ester, 248 g (1.79 mol) of potassium carbonate, and 1350 ml of dimethylformamide is heated to 80° C. for 3 h with stirring. The mixture is then poured out slowly into a mixture of 2300 ml of water and 250 ml of acetic acid. The product is extracted with dichloromethane. The solvent is removed by evaporation.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04822729 |
|---|
| 출처 데이터셋 | uspto-grants-1989_04 |
|---|
| ORD ID | ord-8e1268a3ad914c10b3412d4df8d51779 |
|---|
| 출처 메모 | uspto-grants-1989_04 |
|---|
