Benzenepropanoyl chloride → HCID 1787923, 화합물
반응식
[C:1]([O:5][CH3:6])(=[O:4])[NH:2][NH2:3].[C:7]1([CH2:13][CH2:14][C:15](Cl)=[O:16])[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=1>C(#N)C>[C:7]1([CH2:13][CH2:14][C:15]([NH:3][NH:2][C:1]([O:5][CH3:6])=[O:4])=[O:16])[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=1참가 물질
4
실험 절차
To a solution of 18 g. (0.2 moles) of methyl carbazate and 100 ml. of acetonitrile 33.7 g. (0.2 moles) of β-phenyl-propionyl chloride are added dropwise. The reaction mixture is heated to boiling for 15 hours, clarified and cooled. The crystals are filtered off. Thus 36.85 g. of the desired compound are obtained, yield 80.7%, m.p.: 118° C.
후처리
- temperatureThe reaction mixture is heated
- temperaturecooled
- filtrationThe crystals are filtered off
출처 및 근거
- ORD 기록
- ord-e825e9d503154cf98f041cb3298fda70
- 출처 데이터셋
- uspto-grants-1989_04
- 특허 번호
- US04824670
반응 노트
불러오는 중…