Methyl Acetate → HCID 178517942, 화합물
반응식
[NH2:1][C:2]1[N:3]([C:13](=[O:15])[NH2:14])[N:4]=[CH:5][C:6]=1[C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=1.[C:16](OC)(=O)C>C([O-])([O-])OCC>[OH:15][C:13]1[N:3]2[N:4]=[CH:5][C:6]([C:7]3[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=3)=[C:2]2[N:1]=[CH:16][N:14]=1참가 물질
4
실험 절차
A mixture of 3-amino-2-carbamoyl-4-phenylpyrazole (4.8 g) and ethyl orthoformate (30 ml) is stirred at 100°-110° C. for 13 hours, and thereto is added methanol acetate. The precipitate is separated by filtration, washed with methanol or ethyl acetate, and dried to give the title compound (2.08 g).
후처리
- customThe precipitate is separated by filtration
- washwashed with methanol or ethyl acetate
- customdried
출처 및 근거
- ORD 기록
- ord-21f859648a004f49b76a4d80906220aa
- 출처 데이터셋
- uspto-grants-1989_04
- 특허 번호
- US04824834
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