Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Water → Acetophenone
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | Cumene | HCID 7406 | — |
| 반응물 | 1,4-Diisopropylbenzene | HCID 7486 | — |
| 반응물 | 2-Phenyl-2-propanol | HCID 12053 | — |
| 생성물 | Acetophenone | HCID 7410 | — |
| 생성물 | Cumen hydroperoxide | HCID 53627471 | — |
반응 단계
Using 79.9 g (0.665 mole) of cumene in lieu of p-diisopropylbenzene, oxidation was carried out in the same apparatus and under the same conditions as those employed in Example 1. The reaction product obtained subsequent to its water washing and drying was an oily matter whose weight was 79.6 g. According to results of a high-performance liquid chromatographic analysis, the oily matter was found to contain 3.1 g (0.026 mole; conversion: 96.1%) of cumene and 75.3 g (0.553 mole; yield: 83.2 mole %) of dimethylphenylcarbinol. Acetophenone or cumene hydroperoxide was not formed practically.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04825007 |
| 출처 데이터셋 | uspto-grants-1989_04 |
| ORD ID | ord-2fb7bffb1d064be3b513c787f38a15b1 |
| 출처 메모 | uspto-grants-1989_04 |