참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 2,3-Quinolinedicarboxylic acidtrihydrate | HCID 15558314 | — |
| 용매 | Acetic Anhydride | HCID 7918 | — |
| 생성물 | Furo[3,4-b]quinoline-1,3-dione | HCID 4325463 | — |
반응 단계
A mixture of 2,3-quinolinedicarboxylic acidtrihydrate (0.141 mol) in acetic anhydride (125 mL) is heated at 85° C. for 1/2 hour and then at 100° C. for 1 hour. The reaction mixture is then cooled to room temperature, filtered and the solids washed with ethyl ether to afford the desired 2,3-quinolinedicarboxylic anhydride, mp 225°-228° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04769462 |
|---|
| 출처 데이터셋 | uspto-grants-1988_09 |
|---|
| ORD ID | ord-179810233d824550a3d5f22bdfb74c0b |
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| 출처 메모 | uspto-grants-1988_09 |
|---|
