Nitric Acid → HCID 21421760, 화합물

HRID 622313

반응식

HRID 622313 반응식
[C:1]1([CH:7]([N:9]2[C:13]([C:14]([O:16][CH2:17][CH3:18])=[O:15])=[CH:12][N:11]=[CH:10]2)[CH3:8])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[N+:19]([O-:22])([OH:21])=[O:20]>CC(=O)C>[N+:19]([O-:22])([OH:21])=[O:20].[C:1]1([CH:7]([N:9]2[C:13]([C:14]([O:16][CH2:17][CH3:18])=[O:15])=[CH:12][N:11]=[CH:10]2)[CH3:8])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

참가 물질

4

반응물 2

HCID 944Nitric AcidHCID 36339Ethnor

생성물 1

HCID 21421760HCID 21421760, 화합물

시약·촉매·용매 1

HCID 180Acetone용매

실험 절차

To a solution of 12.2 parts of ethyl 1-(1-phenylethyl)-1H-imidazole-5-carboxylate in 160 parts of 2-propanone were added 5 parts of a nitric acid solution 65%. The product solidifies on scratching, yielding 14 parts of ethyl 1-(1-phenylethyl)-1H-imidazole-5-carboxylate mononitrate; mp. 138°-139° C. (compound 1.146).

출처 및 근거

ORD 기록
ord-fd17da97d4d7482c817be3ac7ed7d2a0
출처 데이터셋
uspto-grants-1988_09
특허 번호
US04770689

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