참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Cyanuric chloride | HCID 7954 | — |
| 반응물 | Sodium Bicarbonate | HCID 516892 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | 2,4-Dichloro-6-methoxy-3,5-triazine | HCID 19267 | — |
반응 단계
7 parts of sodium hydrogencarbonate was added to 50 parts of methanol. This mixture was cooled to 0° C. from outside. Then, 15 parts of cyanuric chloride was added to conduct a reaction for 60 minutes (First condensation). To the reaction mixture was added 100 parts of ice water, and the crystal precipitated was collected by filtration to obtain 2-methoxy-4,6-dichloro-1,3,5-triazine.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 특허 번호 | US04771132 |
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| 출처 데이터셋 | uspto-grants-1988_09 |
|---|
| ORD ID | ord-746073f0754f43e5a068c64e1aa9eb68 |
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| 출처 메모 | uspto-grants-1988_09 |
|---|