Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Thiophenol → Diphenyl sulfide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Thiophenol | HCID 7969 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | Diphenyl sulfide | HCID 8766 | — |
반응 단계
A mixture of bis(dineophyl-orthotrifluoromethylphenyltin)oxide (6.0 g, 5.6 mmol) prepared in Example 6, thiophenol (1.2 g, 11.2 mmol) and toluene (40 g) was treated with the procedure described in Example 7. The product was recrystallized from n-hexane to obtain 5.2 g of dineophylorthotrifluoromethylphenyltin phenylsulfide as a white solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04774235 |
| 출처 데이터셋 | uspto-grants-1988_09 |
| ORD ID | ord-7087eac787814b4481a45eda5fa3f06b |
| 출처 메모 | uspto-grants-1988_09 |