Butyryl chloride → HCID 67509689, 화합물

HRID 623559노트

반응식

HRID 623559 반응식
Cl.[NH2:2][C:3]1[CH:4]=[C:5]([CH:10]=[CH:11][N:12]=1)[C:6]([O:8][CH3:9])=[O:7].[C:13](Cl)(=[O:17])[CH2:14][CH2:15][CH3:16]>>[C:13]([NH:2][C:3]1[CH:4]=[C:5]([CH:10]=[CH:11][N:12]=1)[C:6]([O:8][CH3:9])=[O:7])(=[O:17])[CH2:14][CH2:15][CH3:16]

참가 물질

3

반응물 2

HCID 8855Butyryl chlorideHCID 67509862methyl 2-aminoisonicotinate hydrochloride（WS204501）

생성물 1

HCID 67509689HCID 67509689, 화합물수율 82%

실험 절차

The title compound is prepared in 82% yield (1.94 g, a white solid) from methyl 2-aminoisonicotinate hydrochloride (2.00 g, 10.6 mmol) and butyryl chloride by the similar manner in Step-1 of Carboxylic acid-1.

출처 및 근거

ORD 기록
ord-a0be20038da74f918955558978707c20
출처 데이터셋
uspto-grants-2016_04
특허 번호
US09302991B2

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