6-Methoxy-1H-indole → 3-(2-bromoethyl)-6-methoxy-1H-indole

HRID 624052노트

반응식

HRID 624052 반응식
[Br:1][CH2:2][CH2:3][C:4]1[C:12]2[C:7](=[CH:8][CH:9]=[C:10](OC)[CH:11]=2)[NH:6][CH:5]=1.[CH3:15][O:16]C1C=C2C(C=CN2)=CC=1>>[Br:1][CH2:2][CH2:3][C:4]1[C:12]2[C:7](=[CH:8][C:9]([O:16][CH3:15])=[CH:10][CH:11]=2)[NH:6][CH:5]=1

참가 물질

3

반응물 2

HCID 766596-Methoxy-1H-indoleHCID 111078683-(2-bromoethyl)-5-methoxy-1H-indole

생성물 1

HCID 117368993-(2-bromoethyl)-6-methoxy-1H-indole

실험 절차

The title compound was synthesized according to above mentioned procedure for 3-(2-bromoethyl)-5-methoxy-1H-indole, starting with 6-methoxyindole yielding a brown oil which was stored in the freezer. LC-MS conditions B: tR=0.81 min, [M+H]+=254.13.

출처 및 근거

ORD 기록
ord-af94cd4df54d4c02ab77e2b12c24e8e2
출처 데이터셋
uspto-grants-2016_04
특허 번호
US09303023B2

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