Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acrylonitrile → 3-Cyclohexene-1-carbonitrile, 3,4-dimethyl-
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acrylonitrile | HCID 7855 | — |
| 반응물 | 2,3-Dimethyl-1,3-butadiene | HCID 10566 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | 3-Cyclohexene-1-carbonitrile, 3,4-dimethyl- | HCID 11137219 | 87% |
반응 단계
A solution of acrylonitrile (1 eq.) and 2,3-dimethylbuta-1,3-diene (1.1 eq.) in toluene (2M) was pumped through a heated coil reactor at 240° C. with a residence time of 10 minutes. The resulting mixture was concentrated under reduced pressure and yielded the product as colorless oil (87% yield).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09303232B2 |
| 출처 데이터셋 | uspto-grants-2016_04 |
| ORD ID | ord-b54ff47562704e93b1e2067e66822843 |
| 출처 메모 | uspto-grants-2016_04 |