Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-[(2-Nitrophenyl)sulfanyl]benzoic acid → 2-((2-Aminophenyl)thio)benzoic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-[(2-Nitrophenyl)sulfanyl]benzoic acid | HCID 376978 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 용매 | Ethyl Acetate | HCID 8857 | — |
| 생성물 | 2-((2-Aminophenyl)thio)benzoic acid | HCID 10955828 | — |
반응 단계
To a solution of 2-((2-nitrophenyl)thio)benzoic acid, prepared as described in the previous step, (43.3 g, 0.157 mol) in ethyl acetate (500 mL) was added Pd/C (8 g). The reaction solution was stirred at room temperature overnight under hydrogen gas atmosphere. The mixture was filtered and concentrated to provide the title compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09304126B2 |
| 출처 데이터셋 | uspto-grants-2016_04 |
| ORD ID | ord-91e47b447afe49b2be3082fc09c284fa |
| 출처 메모 | uspto-grants-2016_04 |