Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Glucaric Acid → Adipic Acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Glucaric Acid | HCID 33037 | — |
| 반응물 | Galactaric acid | HCID 3037582 | — |
| 촉매 | Rhenium | HCID 23947 | — |
| 생성물 | Adipic Acid | HCID 196 | — |
반응 단계
Further, as described above, the starting material (glucaric acid or galactaric acid), rhenium catalyst, and acid catalyst are added to the reaction solvent, and reacted together at a proper temperature for a proper reaction time, then separated and purified with a conventional method (e.g., purification with silica column) to obtain glucaric acid ester or galactaric acid ester as an intermediate of adipic acid. In one embodiment, the reaction temperature ranges from 100 to 200° C., and the reaction time is 12 to 24 hours.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09447012B2 |
| 출처 데이터셋 | uspto-grants-2016_09 |
| ORD ID | ord-e4d92eb81e1047428d952ffc9a9ab295 |
| 출처 메모 | uspto-grants-2016_09 |