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(S)-N-((S)-1-(3-isopropylphenyl)ethyl)-2-methylpropane-2-sulfinamide → (1S)-1-[3-(Methylethyl)phenyl]ethylamine

HRID 626397
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HRID 626397 반응식
[CH:1]([C:4]1[CH:5]=[C:6]([C@@H:10]([NH:12][S@](C(C)(C)C)=O)[CH3:11])[CH:7]=[CH:8][CH:9]=1)([CH3:3])[CH3:2]>CO>[CH:1]([C:4]1[CH:5]=[C:6]([C@@H:10]([NH2:12])[CH3:11])[CH:7]=[CH:8][CH:9]=1)([CH3:3])[CH3:2]
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참가 물질

3

반응물 1

HCID 86732637(S)-N-((S)-1-(3-isopropylphenyl)ethyl)-2-methylpropane-2-sulfinamide

생성물 1

HCID 86674570(1S)-1-[3-(Methylethyl)phenyl]ethylamine

시약·촉매·용매 1

HCID 887Methanol용매

실험 절차

The mixture of (S)—N—((S)-1-(3-isopropylphenyl)ethyl)-2-methylpropane-2-sulfinamide (6.1 g, 0.023 mol) in methanol was stirred at room temperature for 3 hours and then concentrated and evaporated with toluene for three times to give the titled compound which was without purification for next step.

후처리

  1. concentrationconcentrated
  2. customevaporated with toluene for three times

출처 및 근거

ORD 기록
ord-6aa35cfe6d984e308516c2debcf98c03
출처 데이터셋
uspto-grants-2016_04
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US09309227B2

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