Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-Bromo-4-chloropyridine → 5-Bromo-4-chloropyridine-3-carbaldehyde
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-Bromo-4-chloropyridine | HCID 817696 | — |
| 반응물 | 4,5-Dichloropyridine-3-carbaldehyde | HCID 59596580 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | 5-Bromo-4-chloropyridine-3-carbaldehyde | HCID 71742307 | 73% |
반응 단계
Following the procedure described for 4,5-dichloropyridine-3-carbaldehyde, 3-bromo-4-chloropyridine and DMF were reacted to afford the title compound as a white solid (3.74 g, 73% yield). 1H NMR (300 MHz, CDCl3): δ 10.48 (d, J=0.4 Hz, 1H), 8.95-8.92 (m, 2H).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09309240B2 |
| 출처 데이터셋 | uspto-grants-2016_04 |
| ORD ID | ord-6dc8ca6f55e846a2a23bc86ea847bcb5 |
| 출처 메모 | uspto-grants-2016_04 |